文献类型：期刊文献

中文题名：咳喘灵贴膏质量标准研究

英文题名：Study on Quality Standard for Kechuanling Plaster

作者：郭玫[1];余晓晖[1];陈卫林[1];李燕燕[1];刘世琼[1]

第一作者：郭玫

机构：[1]甘肃中医学院药学系,甘肃兰州730000

第一机构：甘肃中医药大学药学院（西北中藏药协同创新中心办公室）

年份：2006

卷号：13

期号：3

起止页码：47

中文期刊名：中国中医药信息杂志

外文期刊名：Chinese Journal of Information on Traditional Chinese Medicine

收录：CSTPCD;;CSCD:【CSCD_E2011_2012】；

基金：甘肃省科学事业费资助(QS002-C33-008)

语种：中文

中文关键词：咳喘灵贴膏;α-细辛醚;薄层色谱法;高效夜相色谱法

外文关键词：KechuanlingPlaster; α-asarone； TLC； HPLC

摘要：目的建立咳喘灵贴膏的质量标准。方法采用薄层色谱法鉴别白芥子;采用高效液相色谱法测定石菖蒲中α-细辛醚的含量。结果在薄层色谱中可检出白芥子;α-细辛醚在0.132～0.308μg范围内线性关系良好,r=0.9999,平均加样回收率为101.7%,RSD=2.0%。结论该方法操作简便、快速、准确、重现性好,可用于该制剂的质量控制。
Objective To establish the quality control standard of Kechuanling Plaster. Methods Semen sinapis in Kechuanling Plaster was identified by TLC. The content of a-asarone in Kechuanling Plaster was identified by HPLC. Rusults Semen sinapis in Kechuanling Plaster could be detected by TLC α-asarone shows a good linear relationship at range of 0.132 - 0.308 μg （r=0.9999）. The average recovery was 101.7% and RSD was 2.0%. Conclusion The method was simple, specific and accurate. This study provide a method for the quality control of Kechuanling Plaster.