文献类型：期刊文献

中文题名：当归不同提取方法提取物中挥发性成分比较研究

英文题名：Comparative analysis of volatile compounds in Angelica Sinensis by different acquisition methods with GC-MS technique

作者：王希梅[1];赵泽军[1];张[1];师霞[1];程芳[2];郭玫[1,3];文喜艳[1]

第一作者：王希梅

机构：[1]甘肃中医药大学,甘肃兰州730000;[2]甘肃中医药大学附属医院中药炮制工程中心,甘肃兰州730000;[3]甘肃省中药药理与毒理学重点实验室,甘肃兰州730000

第一机构：甘肃中医药大学

年份：2018

卷号：37

期号：1

起止页码：61

中文期刊名：中兽医医药杂志

外文期刊名：Journal of Traditional Chinese Veterinary Medicine

基金：甘肃省中药药理与毒理学重点实验室开放基金项目(ZDSYS-KJ-2015-003);甘肃中医药大学研究生创新基金(2016CX25)

语种：中文

中文关键词：岷当归;挥发油;水蒸汽蒸馏法;超临界二氧化碳萃取法;微波提取法;气相色谱-质谱联用

外文关键词：Angelica Sinensis; volatile oil; steam distillation; supercritical CO2 fluid extraction; microwave assistedextraction; GC-MS

摘要：目的：比较甘肃岷县产当归不同提取方法中挥发油化学成分的差异。方法：采用超临界CO2流体萃取法（SFE）、水蒸汽蒸馏法（SD）和微波提取法（MAE）提取当归挥发油,结合GC-MS技术对其进行成分分析。结果：3种提取方法对当归挥发油成分的影响较大,其中从水蒸汽提取当归挥发油中鉴定出32种成分,超临界流体提取物中鉴定出54种成分,以上两种方法得到以往文献中未提及的3-（1,5-二甲基-4-己烯基）-6-亚甲基-环己烯等组分,而从微波提取物中鉴定出30种成分。结论：该结果可为岷县当归的进一步研究提供依据。
Objective：To compare the difference of volatile compounds in Angelica Sinensis with different acquisition methods.Methods：The volatile constituents were extracted from Angelica Sinensis by microwave assisted extraction,supercritical CO_2 fluid extraction and steam distillation,using GC-MS to analyze its chemical composition. Results：Different acquisition methods had an obvious influence on volatile oil chemical composition,the volatile oil using vapor distillation method included 32 kinds of chemical composition,and the method of SFE identified 54 kinds of chemical composition. The two methods above got the composition of 3-（1,5-dimethyl-4-hexene）-6-methylene-cyclohexene and other components,which had not addressed in the literature. Meanwhile,the method of microwave extraction identified 30 kinds of ingredients. Conclusion：The results can provide a basis for further study of Angelica Sinensis in Min County.