详细信息

当归不同药用部位近红外漫反射光谱指纹图谱研究    

NIR Fingerprints of Different Medicinal Parts of Angelicae Sinensis Radix

文献类型:期刊文献

中文题名:当归不同药用部位近红外漫反射光谱指纹图谱研究

英文题名:NIR Fingerprints of Different Medicinal Parts of Angelicae Sinensis Radix

作者:张亚亚[1];顾志荣[1,2];丁军霞[1];王耀鹏[1];孙宇靖[1,2];王亚丽[1,2]

第一作者:张亚亚

机构:[1]甘肃中医学院科研实验中心/甘肃省高校中(藏)药化学与质量研究省级重点实验室;[2]甘肃中医学院当归研究所

第一机构:甘肃中医药大学科研实验中心(甘肃省中医药标准化技术委员会秘书处)

年份:2015

卷号:0

期号:7

起止页码:1413

中文期刊名:中药材

外文期刊名:Journal of Chinese Medicinal Materials

收录:MEDLINE(收录号:26946837);CSTPCD;;Scopus;北大核心:【北大核心2014】;CSCD:【CSCD2015_2016】;PubMed;

基金:国家自然科学基金(30960037);甘肃省发改委战略新兴产业和产业技术研究与开发专项项目(2011年);甘肃省科技厅科技支撑计划(144FKCA078)

语种:中文

中文关键词:当归;近红外漫反射光谱;指纹图谱;偏最小二乘判别分析

外文关键词:Angelicae Sinensis Radix; Near-infrared diffuse reflectance spectroscopy; Fingerprint; Partial least square discriminant analysis;

摘要:目的:研究当归不同药用部位的近红外漫反射光谱(NIR)指纹图谱特征。方法:采集甘肃及云南共14个主产县的96批当归样本,以积分球漫反射方式采集NIR指纹图谱,采用相似度分析和偏最小二乘判别分析(PLS-DA)进行研究。结果:当归不同药用部位NIR指纹图谱的平均光谱有一定差异,特征吸收处吸光度大小为归身〉归尾〉归头〉全归;当归不同药用部位NIR指纹图谱的相似度多大于0.95;可以采用PLS-DA模型对当归不同药用部位进行明确的分类;当归不同药用部位NIR指纹图谱的差异主要表现在8 443-8 284 cm^-1、7 003-6 896cm^-1、6 102-5 864 cm^-1、4 847-4 674 cm^-1以及4 386-4 208 cm^-1波数范围内。结论:当归不同药用部位化学成分具有一定的差异。
Objective: To investigate the spectrum characteristics of near-infrared diffuse reflectance spectroscopy( NIR) fingerprint of different medicinal parts of Angelicae Sinensis Radix. Methods: 96 batches of samples were collected from 14 counties of Gansu Province and Yunnan Province. The NIR fingerprints were collected by integrated sphere. Similarity analysis and partial least square discriminant analysis( PLS-DA) were used to analyze the fingerprint. Results: The average spectrum of NIR fingerprint of different medicinal parts of Angelicae Sinensis Radix showed some differences; the absorbance in characteristic absorption was in a decreasing order of body tail head whole. Most NIR fingerprint similarities of different medicinal parts of Angelicae Sinensis Radix exceeded 0. 95. The established model of PLS-DA could be used to accurately classify the medicinal parts of Angelicae Sinensis Radix. The differences of NIR fingerprints of different medicinal parts of Angelicae Sinensis Radix were mainly existing in the wave number ranges of 8 443 - 8 284cm^- 1,7 003 - 6 896 cm^- 1,6 102 - 5 864 cm^- 1,4 847 - 4 674 cm^- 1,and 4 386 - 4 208 cm^- 1. Conclusion: The different medicinal parts of Angelicae Sinensis Radix have some differences in chemical components.

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