详细信息

基于指标成分与近红外光谱对不同贮藏期新品种当归的质量研究    

Quality Study of New Varieties of Angelica sinensis in Different Storage Periods based on Index Components and Near-infrared Spectroscopy

文献类型:期刊文献

中文题名:基于指标成分与近红外光谱对不同贮藏期新品种当归的质量研究

英文题名:Quality Study of New Varieties of Angelica sinensis in Different Storage Periods based on Index Components and Near-infrared Spectroscopy

作者:侯嘉[1];郭鸿儒[2];杜弢[1];王艳[1];王明伟[1]

第一作者:侯嘉

机构:[1]甘肃中医药大学药学院/甘肃省中药质量与标准研究重点实验室培育基地/甘肃省高校中(藏)药化学与质量研究省级重点实验室,甘肃兰州730000;[2]兰州工业研究院,甘肃兰州730070

第一机构:甘肃中医药大学科研实验中心(甘肃省中医药标准化技术委员会秘书处)|甘肃中医药大学药学院(西北中藏药协同创新中心办公室)

年份:2020

期号:3

起止页码:564

中文期刊名:中药材

外文期刊名:Journal of Chinese Medicinal Materials

收录:CSTPCD;;Scopus;北大核心:【北大核心2017】;PubMed;

基金:甘肃省高等学校科研项目(2015B-072);甘肃省中药质量与标准研究重点实验室培育基地开放基金(ZYZL18-001);2015年甘肃省第八批科技计划项目(B类);国家名贵中药资源可持续能力建设子课题(2060302);现代农业产业技术体系建设专项资金(CARS-21)

语种:中文

中文关键词:当归;新品种;指标成分;近红外光谱;贮藏期

外文关键词:Angelica sinensis(Oliv.)Diels;New varieties;Index components;Near-infrared spectroscopy;Storage period

摘要:目的:考察新品种当归贮藏后质量的稳定性及适宜贮藏期,为新品种当归的养护及贮藏提供理论依据,进一步为新品种当归的市场推广奠定基础。方法:选取当归新品种岷归1号、岷归2号、岷归4号和岷归5号,分别贮藏不同的时间(6、12、36个月)后,用HPLC测定4种指标成分(阿魏酸、洋川芎内酯H、洋川芎内酯I及藁本内酯),并结合新品种当归的近红外光谱对其进行比较研究。结果:新品种当归贮藏12个月后,阿魏酸及藁本内酯的含量无显著变化,而贮藏36个月后阿魏酸、藁本内酯的含量显著降低,其中阿魏酸的含量低于药典标准;洋川芎内酯H和洋川芎内酯I的含量呈随贮藏时间延长而增加的趋势。通过对新品种当归的近红外光谱建模,能很好地区分贮藏6、12、36个月的新品种当归药材。结论:选育的新品种当归贮藏期不能超过36个月。选育品种和贮藏期都能影响当归药材的质量,且贮藏期对其影响更显著。通过近红外光谱法可以直观、有效地对不同贮藏期的新品种当归药材进行定性鉴别。
Objective:To investigate the stability and suitable storage period of new varieties of Angelica sinensis,so as to provide the theoretical basis for the conservation and storage of the new varieties of Angelica sinensis and further lay the foundation for the market promotion of the new variety of Angelica sinensis.Methods:Four new varieties of Angelica sinensis(Mingui 1,Mingui 2,Mingui 4 and Mingui 5)were selected and stored for 6,12 and 36 months,respectively.Four index components(ferulic acid,senkyunolide H,senkyunolide I and ligustilide)in new varieties of Angelica sinensis were determined by HPLC,and the near-infrared spectroscopy of the new varieties of Angelica sinensis was used to make a comparative study.Results:After 12 months of storage of new varieties of Angelica sinensis,the contents of ferulic acid and ligustilide did not change significantly,while their contents decreased significantly after 36 months of storage,and the content of ferulic acid was lower than that of pharmacopoeia.The contents of senkyunolide H and senkyunolide I increased with the increase of storage time.The samples of new varieties of Angelica sinensis stored in 6,12 and 36 months could be distinguished by near-infrared spectroscopy modeling.Conclusion:The storage period of selected new varieties of Angelica sinensis should not exceed 36 months.Both breeding varieties and storage period can affect the quality of Angelica sinensis,and the effect of storage period is more significant.Near-infrared spectroscopy can be used to intuitively and effectively identify the new varieties of Angelica sinensis in different storage periods.

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